In-situ X-ray Absorption Spectroscopy (XAS) Cell

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In-situ X-ray Absorption Spectroscopy (XAS) Cell

In-situ X-ray Absorption Spectroscopy (XAS) Cell

Product Description
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n-situ X-ray Absorption Spectroscopy (XAS / XAFS) Electrochemical Cell

Real-Time Electronic Structure Probing · Synchrotron-Compatible · Modular Architecture

Product Overview
The FrankLab In-situ X-ray Absorption Spectroscopy (XAS / XAFS) Electrochemical Cell is a precision-engineered reactor designed for real-time investigation of electronic structure, oxidation states, and local coordination environments of electrode materials during electrochemical operation.
Optimized for synchrotron-based XAS/XAFS experiments, this platform enables simultaneous electrochemical control and X-ray transmission or fluorescence detection, allowing researchers to directly correlate electrochemical performance with atomic-scale structural evolution.
The cell features a replaceable X-ray transparent window, chemically resistant construction, and modular configurations supporting single-cell and dual-cell (H-type) electrochemical reactions.

Available Models & Configurations
XAFS-1 | Single-Chamber In-situ XAS Cell
•Compact single-cell configuration
•Ideal for liquid-phase electrochemical XAS studies
•Simple assembly and fast beamline alignment
XAFS-2 | Dual-Chamber (H-Type) In-situ XAS Cell
•Cathode and anode separated by a replaceable membrane
•Minimizes cross-interference between redox reactions
•Suitable for mechanistic and durability studies


Structural Design & Materials
Chemically Robust Cell Body
•Main body fabricated from high-purity PEEK
•Excellent resistance to acids, bases, and organic electrolytes
•Stable under prolonged synchrotron irradiation
X-ray Transparent Observation Window
•Standard window material: Kapton® (Polyimide) film
•Optimized for X-ray transmission and minimal background scattering
•Window materials interchangeable for different beamline requirements
Modular Architecture
•Supports two-electrode or three-electrode configurations
•Working electrode geometry and size customizable
•Cell volume configurable upon request

Technical Specifications
Parameter Specification
Cell type In-situ XAS / XAFS electrochemical cell
Compatible techniques XANES, EXAFS, operando XAS
Cell body material PEEK
Window material Kapton® (standard)
Window configuration Replaceable, beamline-compatible
Electrode system 2-electrode or 3-electrode
Membrane option Replaceable ion-exchange membrane (XAFS-2)
Electrolyte handling Static or flow-through
Assembly Tool-assisted quick assembly
Cleaning Fully disassemblable components
Supported Electrode Configurations
Working Electrode
•Custom-designed based on experimental needs
•Compatible with thin films, foils, coated substrates, and catalyst layers
Reference Electrode
•Ag/AgCl or Ag⁺ (optional)
•Custom reference configurations available
Counter Electrode
•Platinum wire (standard)
•Other materials available upon request

Key Advantages
•True Operando XAS Capability Simultaneously probes electronic structure and electrochemical behavior under realistic operating conditions.
• Beamline-Friendly Design Compact geometry, X-ray transparent window, and low background signal ensure high data quality at synchrotron facilities.
• Modular & Expandable Platform Single-cell, H-type, and gas-phase configurations cover a wide range of electrochemical research needs.
• Chemical & Mechanical Stability PEEK construction ensures long-term durability in harsh electrochemical environments.
• Research-Grade Reproducibility Precisely machined interfaces and sealing structures support consistent, repeatable measurements.

Typical Applications
•Operando XANES / EXAFS of electrocatalysts
•Valence state evolution during redox reactions
•Structural dynamics in battery and supercapacitor materials
•CO₂ reduction and gas-electrochemistry under X-ray probing
•Catalyst degradation and reconstruction studies

Standard Package Contents
•In-situ XAS electrochemical cell body (selected model)
•X-ray transparent Kapton® window
•Sealing gaskets and fasteners
•Standard electrode ports and fittings
(Electrodes, membranes, and gas tubing sold separately)

Customization Options (On Request)
•Alternative X-ray window materials
•Custom electrode geometries
•Flow-through electrochemical configurations
•High-temperature or pressure-optimized designs
•Full beamline integration support

 

For Custom Orders or Inquiries

If you have custom requirements or any additional questions, feel free to contact us:

Email: support@franklab.shop

FrankLab offers worldwide shipping.Orders are normally shipped from our facility in Hangzhou, China within 1-2 business days after the payment is made. It is very important that the correct shipping address is entered at checkout. We are not responsible for incorrect or undeliverable addresses.

 

Shipping Fees

Orders below USD 499 : Shipping fee of USD 14.90

Orders USD 499 and above: Free worldwide shipping

 

Large Orders & Bulk Discounts

For orders over USD 3,000, please contact our customer support team to check special pricing or potential bulk discounts before placing your order.

IMPORTANT: All goods must be inspected immediately upon delivery. Any shipping damage, missing items, or product defects must be reported to both Franklab team and the shipping carrier within 24 hours of delivery. Failure to report issues within this timeframe may result in your claim being denied. Please retain all original packaging materials, as they may be required for filing a damage claim. 

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For shipping, returns, or bulk order inquiries, please contact:
support@franklab.shop

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