In-situ XRD Electrochemical Cell

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In-situ XRD Electrochemical Cell

In-situ XRD Electrochemical Cell

Product Description
Shipping & Delivery
Product Overview
The FrankLab In-situ XRD Electrochemical Cell is a precision-engineered electrochemical reactor designed for real-time X-ray diffraction (XRD) characterization of electrode materials during electrochemical operation.
By positioning the working electrode directly beneath an X-ray transparent window, this cell enables operando monitoring of phase transitions, lattice evolution, crystallinity changes, and reaction-induced structural dynamics under applied potential or current.
Unlike conventional electrochemical cells, this platform is optimized for low absorption, short beam path, and minimal parasitic scattering, making it suitable for laboratory XRD systems and synchrotron beamlines.

Structural Design & Measurement Concept
True In-situ XRD Geometry
•Working electrode (WE) positioned directly below the X-ray window
•X-ray beam passes vertically through the window onto the electrode surface
•Reflected / diffracted signal collected without cell disassembly
Low-Loss Optical Path
•Ultra-short WE-to-window distance (< 6 mm) minimizes beam attenuation
•Optimized chamber depth reduces electrolyte absorption and background noise
Compact, Symmetric Cell Architecture
•Square, rigid body minimizes mechanical drift
•Uniform compression ensures stable electrode positioning during long scans

Materials & Construction
Cell Body
•High-purity PEEK (Polyether Ether Ketone)
•Reinforced with high-purity titanium components
•Chemically resistant to acidic, alkaline, and organic electrolytes
X-ray Window
Polyimide (PI) window (standard)
•Excellent X-ray transparency
•Low background scattering
•High mechanical flexibility
Alternative window materials available on request (e.g., Kapton® variants)

Electrode Configuration
Standard Three-Electrode System
Working electrode (WE)
•Standard: 5 mm glassy carbon disk
•Compatible with: Au, Pt, Ag, graphite, metal disks, custom substrates
Reference electrode (RE)
•Ag/AgCl (standard)
•Optional: Ag⁺ reference
Counter electrode (CE)
•Platinum wire (standard)
✔ Disk-type electrodes ensure reproducible diffraction geometry
✔ Custom electrode diameters and materials available

Electrolyte Handling & Operation
•Supports flow-through electrochemical testing
•Also compatible with syringe-based electrolyte injection
•Low internal dead volume for rapid electrolyte exchange
•Suitable for static, pulsed, or dynamic electrochemical protocols

Technical Specifications
Parameter Specification
Cell type In-situ XRD electrochemical cell
Cell body material PEEK + high-purity titanium
X-ray window material Polyimide (PI)
Window thickness Optimized for XRD (low absorption)
Window diameter 25 mm
Distance (WE → window) < 6 mm
Working electrode 5 mm GC disk (standard)
Reference electrode Ag/AgCl (Ag⁺ optional)
Counter electrode Platinum wire
Electrolyte filling Injection or flow mode
Assembly Tool-assisted, modular
Cleaning Fully disassemblable
XRD compatibility Lab XRD & synchrotron systems
Key Advantages
• True Operando XRD Capability
Observe phase evolution, crystallographic transitions, and structural degradation during electrochemical cycling.
• Low Background, High Signal Fidelity
PI window and minimized electrolyte thickness reduce parasitic scattering and absorption.
• Stable Long-Duration Measurements
Rigid PEEK-Ti structure maintains alignment during extended scans and cycling tests.
• Flexible Electrode Platform
Supports metallic, carbon, and functional electrode materials for batteries, catalysts, and corrosion studies.
• Research-Grade Engineering
Designed for repeatability, alignment stability, and compatibility with advanced characterization workflows.

Typical Applications
•Operando XRD of battery electrode materials
•Phase transition studies under electrochemical bias
•Structural evolution of electrocatalysts
•Corrosion and passivation layer formation
•Intercalation / conversion reaction analysis
•Synchrotron-based electrochemical XRD experiments

Standard Package Contents
•In-situ XRD electrochemical cell body
•Polyimide X-ray window
•Glassy carbon working electrode (5 mm)
•Ag/AgCl reference electrode
•Platinum wire counter electrode
•Standard fittings, seals, and fasteners
(Custom electrodes and alternative windows available separately)

Customization Options (On Request)
•Alternative window materials or thickness
•Adjustable WE-to-window distance
•Custom electrode diameters or holders
•Flow-optimized inlet/outlet geometry
•Synchrotron-specific mounting adaptations
•High-temperature or pressure-tolerant variants

For Custom Orders or Inquiries

If you have custom requirements or any additional questions, feel free to contact us:

Email: support@franklab.shop

FrankLab offers worldwide shipping.Orders are normally shipped from our facility in Hangzhou, China within 1-2 business days after the payment is made. It is very important that the correct shipping address is entered at checkout. We are not responsible for incorrect or undeliverable addresses.

 

Shipping Fees

Orders below USD 499 : Shipping fee of USD 14.90

Orders USD 499 and above: Free worldwide shipping

 

Large Orders & Bulk Discounts

For orders over USD 3,000, please contact our customer support team to check special pricing or potential bulk discounts before placing your order.

IMPORTANT: All goods must be inspected immediately upon delivery. Any shipping damage, missing items, or product defects must be reported to both Franklab team and the shipping carrier within 24 hours of delivery. Failure to report issues within this timeframe may result in your claim being denied. Please retain all original packaging materials, as they may be required for filing a damage claim. 

Contact Us

For shipping, returns, or bulk order inquiries, please contact:
support@franklab.shop

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