In-situ XRD Li-ion Test Cell [Three-Electrode]

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Three-Electrode
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In-situ XRD Li-ion Test Cell [Three-Electrode]

In-situ XRD Li-ion Test Cell [Three-Electrode]

Product Description
Shipping & Delivery
Product Overview
The In-situ Raman Electrochemical Cell is a three-electrode, operando-grade test platform engineered for real-time Raman spectroscopy and electrochemical analysis of battery and electrode materials under realistic cycling conditions.
Unlike two-electrode XRD cells, B003-RM integrates a dedicated Ag/AgCl reference electrode, enabling precise potential control, accurate kinetic measurements, and mechanistic electrochemical studies during in-situ optical observation.
Machined from high-purity titanium and equipped with a sapphire optical window positioned < 2 mm from the working electrode, B003-RM delivers exceptional Raman signal quality, mechanical stability, and long-term reproducibility—meeting the standards expected by PI-level research groups, synchrotron users, and advanced battery engineers.

Structural Design & Electrochemical Architecture
True Three-Electrode Configuration
•Working electrode (WE)
•Counter electrode (CE)
•Ag/AgCl reference electrode (RE) ✔ Enables accurate potential referencing and separation of kinetic vs. ohmic effects ✔ Essential for mechanistic Raman-electrochemical studies
Ultra-Close Optical Access
•⌀8 mm sapphire window
•< 2 mm WE-to-window distance
•Optimized for high-signal operando Raman spectroscopy
Pressure-Controlled Stack
•Integrated spring-loaded compression system
•Enables controlled contact pressure
•Ideal for studying interfacial resistance, SEI evolution, and mechanical degradation

Materials & Sealing Integrity
Cell Body
•High-purity titanium
•Excellent chemical resistance to battery electrolytes
•Low background signal for optical spectroscopy
Sealing System
•Chemically resistant O-rings
•Screw-fastened structure for uniform compression
•Gas-tight and electrolyte-stable
Workflow Compatibility
•Fully glovebox compatible
•Can be transferred to ambient or optical platforms after sealing

Key Advantages
•True Three-Electrode Precision Enables reliable potential-controlled Raman measurements, unlike pseudo two-electrode designs.
• Operando Raman-Optimized Geometry Minimal optical path length maximizes Raman signal while reducing fluorescence and scattering losses.
•Pressure-Tunable Interfaces Spring loading allows systematic investigation of contact resistance and mechanical–electrochemical coupling.
• Battery-Relevant Engineering Designed for real cycling—not static demonstrations—supporting long experiments and repeated use.
• Rapid Assembly & Reproducibility Fast disassembly supports quick sample turnover, cleaning, and protocol iteration.

Technical Specifications
Parameter Specification
Model B003-RM
Application In-situ Raman spectroscopy (battery & electrochemical systems)
Electrode configuration Three-electrode (WE / CE / Ag/AgCl RE)
Cell body material High-purity titanium
Optical window Sapphire
Window diameter 8 mm
WE-to-window distance < 2 mm
Load control Spring-loaded pressure adjustment
Sealing mechanism O-rings + screw tightening
Dimensions (L×W×H) 50 × 50 × 24 mm
Assembly environment Glovebox compatible
Operating environment Ambient after sealing
Reusability Fully reusable; easy cleaning
Typical Applications
•Operando Raman studies of Li-ion battery electrodes
•SEI formation and evolution monitoring
•Electrode surface reconstruction during cycling
•Contact resistance and interface degradation analysis
•Fundamental electrochemical–spectroscopic coupling studies

Package Contents
•B003-RM electrochemical cell body
•Sapphire optical window
•Ag/AgCl reference electrode
•Spring-loading compression unit
•Titanium screws and O-ring sealing set
(Working and counter electrodes supplied separately unless specified)

For Custom Orders or Inquiries

If you have custom requirements or any additional questions, feel free to contact us:

Email: support@franklab.shop

FrankLab offers worldwide shipping.Orders are normally shipped from our facility in Hangzhou, China within 1-2 business days after the payment is made. It is very important that the correct shipping address is entered at checkout. We are not responsible for incorrect or undeliverable addresses.

 

Shipping Fees

Orders below USD 499 : Shipping fee of USD 14.90

Orders USD 499 and above: Free worldwide shipping

 

Large Orders & Bulk Discounts

For orders over USD 3,000, please contact our customer support team to check special pricing or potential bulk discounts before placing your order.

IMPORTANT: All goods must be inspected immediately upon delivery. Any shipping damage, missing items, or product defects must be reported to both Franklab team and the shipping carrier within 24 hours of delivery. Failure to report issues within this timeframe may result in your claim being denied. Please retain all original packaging materials, as they may be required for filing a damage claim. 

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For shipping, returns, or bulk order inquiries, please contact:
support@franklab.shop

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