In-situ XRD Li-ion Test Cell [Two-Electrode]

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Two-Electrode
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In-situ XRD Li-ion Test Cell [Two-Electrode]

In-situ XRD Li-ion Test Cell [Two-Electrode]

Product Description
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Product Overview
The In-situ XRD Li-ion Test Cell is a two-electrode operando electrochemical cell engineered for real-time structural and phase evolution studies of battery electrodes during electrochemical cycling.
Built entirely from high-purity titanium, the cell delivers exceptional chemical stability, mechanical robustness, and X-ray compatibility. A sapphire optical/X-ray window positioned extremely close to the working electrode enables high signal-to-noise in-situ XRD and synchrotron measurements, even under dynamic cycling conditions.
A spring-loaded compression system allows precise control of stack pressure, making the B002-XRD particularly suitable for investigating solid–solid interfaces, contact resistance, SEI evolution, and electrode integrity in Li-ion and beyond-Li battery systems.

Structural Design & Engineering
Two-Electrode Architecture
•Designed for battery-relevant configurations
•Supports separator or membrane isolation (user-supplied)
•Minimizes geometric complexity for clean diffraction signals
Ultra-Close Optical Access
•⌀8 mm sapphire window
•< 2 mm distance from working electrode
•Optimized for operando XRD, synchrotron, and optical probing
Pressure-Controlled Stack
•Integrated spring-loaded compression mechanism
•Enables reproducible mechanical pressure on electrode stack
•Critical for studying interfacial stability and contact evolution

Materials & Sealing
Cell Body
•High-purity Titanium
•Excellent resistance to electrolytes and reactive species
•Ideal for long-duration cycling and beamline use
Sealing System
•Chemically resistant O-ring sealing
•Reliable gas-tight performance
•Stable during glovebox assembly and external operation

Key Advantages
•True Operando XRD Capability Enables direct correlation between electrochemical cycling and crystal structure evolution.
• Pressure-Tunable Interface Spring-loaded design allows controlled investigation of mechanical–electrochemical coupling.
• Synchrotron-Compatible Geometry Compact footprint and optimized window placement reduce background scattering.
• Glovebox-to-Ambient Workflow Assemble in glovebox → seal → measure in ambient beamline environments.
• Fast Turnaround Testing Quick assembly/disassembly supports repeated experiments and rapid iteration.

Technical Specifications
Parameter Specification
Model B002-XRD
Application In-situ XRD / optical battery analysis
Electrode configuration Two-electrode
Cell body material High-purity titanium
Window material Sapphire
Optical window diameter 8 mm
WE-to-window distance < 2 mm
Channel width 8 mm
Pressure control Spring-loaded compression
Sealing O-rings + screw fastening
Assembly environment Glovebox compatible
Operating environment Ambient after sealing
Cell dimensions (L×W×H) 50 × 50 × 20 mm
Typical Applications
•Operando XRD of Li-ion battery electrodes
•Phase transition tracking during charge/discharge
•Interfacial stability and SEI evolution studies
•Solid-state and semi-solid battery research
•Synchrotron-based battery characterization

Package Contents
•B002-XRD electrochemical cell body
•Sapphire optical/X-ray window
•Spring compression assembly
•Titanium frame
•O-rings and fastening screws
(Electrodes, separators, and electrolytes not included)

 

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Email: support@franklab.shop

FrankLab offers worldwide shipping.Orders are normally shipped from our facility in Hangzhou, China within 1-2 business days after the payment is made. It is very important that the correct shipping address is entered at checkout. We are not responsible for incorrect or undeliverable addresses.

 

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Orders below USD 499 : Shipping fee of USD 14.90

Orders USD 499 and above: Free worldwide shipping

 

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For orders over USD 3,000, please contact our customer support team to check special pricing or potential bulk discounts before placing your order.

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